Covestro Deutschland Ag

Bayer Materialscience Ag

Cliff Andre Peters

Thomas Knauf

Michael Merkel

Thorsten Schmidt

Karl-Heinz Wilke

The present invention relates to a method for treating a substance mixture comprising an aromatic amine, wherein the aromatic amine is aniline or 2,4-diaminotoluene, preferably aniline. The substance mixture comprises an aromatic amine and compounds having a higher boiling point than the aromatic amine. The method for treating the substance mixture requires I) separating the first substance mixture by means of distillation in a first distillation unit (), to at least partially remove some of the aromatic amine in the process, and to obtain a first bottom product which is removed from the first distillation unit (). After removal from the first distillation unit (), the bottom product is diluted with a condensed top product from a distillation unit that is different from the first distillation unit and/or with a composition that comprises methanol.

Method for treating a substance mixture comprising an aromatic amine, in particular a substance mixture of raw aniline

The present invention relates to a method for producing aromatic amines by the hydrogenation of aromatic nitro compounds. This method supplies aromatic nitro compounds and hydrogen to a reactor and contacts them with a hydrogenation catalyst; and stops the supply of aromatic nitro compounds and hydrogen to the reactor. The supply of aromatic nitro compounds and hydrogen to the reactor is stopped to ensure safe shutdown of the reactor.

Method for stopping a reaction during the production of aromatic amines from nitroaromatics

The present invention relates to a method of producing aromatic amines by hydrogenation of aromatic nitro compounds. This method provides a reactor containing a hydrogenation catalyst; supplies aromatic nitro compounds and hydrogen to the reactor and contacts them with a hydrogenation catalyst, in which the hydrogen which is supplied to the reactor is by a compressor and the compressor contains an operating fluid which at least partially contacts the hydrogen; and regenerates the hydrogenation catalyst by heating and contacting it with oxygen. Particular operating liquids are subsequently exchanged.

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Schmedeswurth, Germany

Cliff Andre Peters