Gaylord Chemical Corporation

Claude A Bloom, Jr

Joe Paul Gibbons, Jr

Alan M Rodger

Charles G Ashe

Kenneth W Otto

John L Ferguson

One aspect of this invention relates to processes for solidifying dimethylsufoxide including the steps of partially solidifying a liquid phase including dimethylsulfoxide and one or more impurities, to form a mixture comprising solid dimethylsulfoxide and a liquid residue, and substantially separating the solid dimethylsulfoxide from the liquid residue, wherein the liquid residue comprises liquid dimethylsulfoxide and at least a portion of the impurities, and wherein the liquid residue is not subsequently treated by any step of partial solidification. In certain embodiments of the processes of the invention, ultra-high purity DMSO that exceeds the purity specifications for U.S.P. grade DMSO can be produced by employing solidification, fractional solidification and/or melt crystallization processes.

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Bogalusa, LA, United States of America

Claude A Bloom, Jr