Taiyen Biotech Co., Ltd.

Taiwan Salt Company

Chen-Hsin Lai

Tzyy-Bin Werng

Chung-Hong Lau

Tsang-Tien Wang

Chih-Hsing Tsao

A method for synthesizing aluminum nitride is disclosed, wherein an ignition agent is formed by mixing an azide powder (such as sodium azide; NaN) and aluminum powder, and is paved on an ignition portion of a reactant-containing body having a plurality of ratios of aluminum to a diluent, wherein the content of the diluent is gradually increased in accordance with the propagation direction of combustion wave generated in the combustion synthesis process. The method for synthesizing aluminum nitride is to ignite the ignition agent located in the ignition portion of the reactant-containing body under an ambience in which the pressure is less than 1 atm, and to introduce nitrogen gas as the nitrogen source into the reaction chamber after ignition.

Method for synthesizing aluminum nitride

A method and an apparatus for preparing aluminum nitride are disclosed. The method for preparing aluminum nitride is first to prepare a reactant-containing body filled with admixtures of aluminum powder, a diluent (aluminum nitride powder) and nitrogen-containing solid compound, the reactant-containing body having an ignition portion, a propagating portion, a sustaining portion and an ending portion. Thereafter, the reactant-containing body is placed on a base having through holes in a reaction chamber, and preheated to a predetermined temperature for a predetermined period of time. Then, a re-circulating nitrogen gas is introduced through the reactant-containing body, and coolant is re-circulated between an inner wall and an outer wall of the reaction chamber, and then the ignition portion is ignited to perform a combustion synthesis process, thereby preparing the aluminum nitride, thereby preparing the aluminum nitride. The apparatus for preparing aluminum nitride comprises a reaction chamber having an inner wall and an outer wall, wherein a coolant is re-circulated between the inner wall and the outer wall; a preheating device; a nitrogen re-circulation system; and an igniting device.

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Tainan, Taiwan

Chen-Hsin Lai