Reading Alloys, Inc.

Cabot Corporation

Brian J Higgins

James W Robison

Charles A Motchenbacher

Thomas J Fonville

Edwin J Bielecki

Roger M Bergman

Karl A Romberger

James D Kahl, Jr, Legal Representative

James D Kahl, Deceased

Jeni L Heenley, Legal Representative

Teri Ann Boyer, Legal Representative

The present invention relates to high-purity niobium monoxide powder (NbO) produced by a process of combining a mixture of higher niobium oxides and niobium metal powder or granules; heating and reacting the compacted mixture under controlled atmosphere to achieve temperature greater than about 1945&#xb0; C., at which temperature the NbO is liquid; solidifying the liquid NbO to form a body of material; and fragmenting the body to form NbO particles suitable for application as capacitor anodes. The NbO product is unusually pure in composition and crystallography, and can be used for capacitors and for other electronic applications. The method of production of the NbO is robust, does not require high-purity feedstock, and can reclaim value from waste streams associated with the processing of NbO electronic components. The method of production also can be used to make high-purity NbOand mixtures of niobium metal/niobium monoxide and niobium monoxide/niobium dioxide. The method further is ideal for doping of the product oxides to enhance particular characteristics of the materials. The method further allows the production of single crystal or directionally-solidified ingots. In contrast to the spongy, highly porous agglomerates produced by other techniques, the present invention produces solid, non-porous ingots that can be fragmented to fine, non-porous angular particles suitable for electronic applications.

Production of high-purity niobium monoxide and capacitor production therefrom

The present invention relates to high-purity niobium monoxide powder (NbO) produced by a process of combining a mixture of higher niobium oxides and niobium metal powder or granules; heating and reacting the compacted mixture under controlled atmosphere to achieve temperatures greater than about 1800&#xb0; C., at which temperature the NbO is liquid; solidifying the liquid NbO to form a body of material; and fragmenting the body to form NbO particles suitable for application as e.g., capacitor anodes. The NbO product is unusually pure in composition and crystallography, highly dense, and can be used for capacitors and for other electronic applications. The method of production of the NbO is robust, does not require high-purity feedstock, and can reclaim value from waste streams associated with the processing of NbO electronic components.

Vanadium-aluminum master alloys with small amounts of refractory metals such as ruthenium, are made substantially free of refractory inclusions and with a substantially homogeneous microstructure by reacting vanadium oxides with excess aluminum through an aluminothermic reduction reaction in the presence of the refractory to yield the desired master alloy. A preferred homogeneous vanadium-aluminum-ruthenium alloy without inclusions contains from about 59 to 70% of vanadium, about 29 to 40% of aluminum, and about 1 to 10% of ruthenium, all based on the weight of the alloy. The substantially homogeneous and inclusion-free master alloy is then used to produce titanium base alloys of higher quality, such as 4% vanadium and 6% aluminum titanium base alloys containing small amounts of refractory metals, usually containing from about 0.1 to 1.0% of ruthenium.

Method for producing vanadium-aluminum-ruthenium master alloys and

Disclosed is a process for dissolving tantalum and/or columbium-containing materials contaminated with alkali metal impurities. The tantalum and columbium materials are digested in a solution comprising hydrofluoric acid and a fluosilicate-containing compound. The alkali metals are reacted to form precipitated fluosilicates, which then can readily be separated.

Process for dissolving tantalum/columbium materials containing alkali

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Reading, PA, United States of America

Brian J Higgins