Heraeus Quarzglas Gmbh & Co Kg

Boris Gromann

Nigel Robert Whippey

Matthias Söhn

Walter Lehmann

Michael Hünermann

Nils Christian Nielsen

Abdoul-Gafar Kpebane

Christian Neumann

Thomas Kayser

Matthias Otter

Christian Schenk

Gerrit Scheich

Martin Arndt

Mirko Wittrin

Kathrin Wissel-Stoll

Markus Wilde

Alexander Blumenau

Heinz Bauscher

Eduard Visnow

Lothar Huefner

Marcus Constantin Göbel

Matthias SÖHN

Marcus Constantin GÖBEL

Bastian Weisenseel

A quartz glass body and a process for the preparation of a quartz glass body is disclosed. One process includes providing a silicon dioxide granulate from a pyrogenic silicon dioxide powder, making a glass melt out of the silicon dioxide granulate and making a quartz glass body out of at least part of the glass melt. In at least one process a silicon component different from silicon dioxide is added. A quartz glass body is obtainable by this process. A light guide, an illuminant and a formed body, are each obtainable by further processing of the quartz glass body.

Increase in silicon content in the preparation of quartz glass

In a method of manufacturing a tube of quartz glass by molding a hollow cylinder having a wall thickness of at least 20 mm, the cylinder is continuously fed under rotation about a rotational axis into a heating zone at a relative feed rate V, softened and radially expanded under the effect of a gas pressure. A tube strand is continuously formed and is withdrawn at a withdrawal rate V. In order to mold thick-walled initial hollow cylinders of quartz glass into tubes with larger diameter, the gas pressure is used as an actuating variable of a diameter regulation for the tube outer diameter or for a geometrical correlated parameter thereof, and in a pressure build-up phase the gas pressure is gradually increased from a lower initial value to a higher final value, and that the following applies to the ratio of Vand V:V=V±0.2·V.

Quartz glass tube and method of manufacturing the same

One aspect relates to a process for the preparation of a quartz glass body, including providing a silicon dioxide granulate, wherein the silicon dioxide granulate was made from pyrogenic silicon dioxide powder and the silicon dioxide granulate has a BET surface area in a range from 20 to 40 m/g, making a glass melt out of silicon dioxide granulate in an oven and making a quartz glass body out of at least part of the glass melt. The oven has at least a first and a further chamber connected to one another via a passage. The temperature in the first chamber is lower than the temperature in the further chambers. On aspect relates to a quartz glass body which is obtainable by this process. One aspect relates to a light guide, an illuminant and a formed body, which are each obtainable by further processing of the quartz glass body.

Preparation of a quartz glass body in a multi-chamber oven

One aspect relates to a process for the preparation of a quartz glass body. The process includes providing silicon dioxide particles, making a glass melt out of the silicon dioxide particles in an oven and making a quartz glass body out of at least part of the glass melt. The oven has a gas outlet through which gas is removed from the oven, wherein the dew point of the gas on exiting the oven through the gas outlet is less than&#xb0; C. One aspect further relates to a quartz glass body which is obtainable by this process. One aspect further relates to a light guide, an illuminant and a formed body, which are each obtainable by further processing of the quartz glass body.

Preparation of quartz glass bodies with dew point monitoring in the melting oven

The invention relates to a process for preparing a quartz glass body comprising the process steps i.) Providing a silicon dioxide granulate, ii.) Making a glass melt from the silicon dioxide granulate in a melting crucible, and iii.) Making a quartz glass body from at least a part of the glass melt, wherein the melting crucible is comprised in an oven and is made of at least one material comprising tungsten or molybdenum or a combination thereof. The invention further relates to a quartz glass body which can be obtained by this process. Further, the invention relates to a light guide, an illuminant and a formed body, each of which can be obtained by processing the quartz glass body further.

Preparation of a quartz glass body in a melting crucible of refractory metal

One aspect relates to a process for the preparation of a quartz glass body, including providing a silicon dioxide granulate, wherein the silicon dioxide granulate was made from pyrogenic silicon dioxide powder and the silicon dioxide granulate has a BET surface area in a range from 20 to 40 m/g, making a glass melt out of silicon dioxide granulate in an oven and making a quartz glass body out of at least part of the glass melt. The oven has at least a first and a further chamber connected to one another via a passage. The temperature in the first chamber is lower than the temperature in the further chambers. One aspect relates to a quartz glass body which is obtainable by this process. One aspect relates to a light guide, an illuminant and a formed body, which are each obtainable by further processing of the quartz glass body.

The invention relates to a process for the preparation of a quartz glass grain comprising the process steps i.) Providing a silicon dioxide granulate from a pyrogenically produced silicon dioxide powder, ii.) Making a glass melt out of silicon dioxide granulate, iii.) Making a quartz glass body out of at least part of the glass melt and iv.) Reducing the size of the quartz glass body to obtain the quartz glass grain. The invention further relates to a quartz glass grain which is obtainable by this process. The invention further relates to opaque quartz glass bodies, which are obtainable by further processing of the quartz glass grain.

Preparation of a synthetic quartz glass grain

A method and apparatus are provided for producing a tube of glass by zonewise heating and softening of a hollow cylinder by a movable heating zone while rotating about its rotation axis. The glass tube is continuously formed by radial expansion of the softened region under action of centrifugal force and/or internal overpressure applied in the hollow-cylinder bore. The method and apparatus make it possible to deform the hollow cylinder in a single or a small number of forming steps into a glass tube having a larger outer diameter and high dimensional accuracy by determining a circumferential position at which the wall thickness is comparatively small, and during heating and softening of the rotating hollow cylinder a coolant is dispensed from a coolant source onto the deformation zone only when or predominantly when the circumferential position having the comparatively small wall thickness passes the coolant source.

Method and apparatus for producing a tube of glass

A method for forming a hollow cylinder, in a single step, into a quartz glass tube with a large outer diameter and high dimensional stability is provided. To produce the tube, the cylinder, while rotating, is softened in portions in a heating zone which is moved at a relative feed rate Va and the softened portion is radially expanded by a centrifugal force and/or internal overpressure applied in the hollow cylinder bore so as to form a deformation zone. The radial expansion of the softened portion is carried out at a location-dependent radial expansion rate Vr, the profile of which along the deformation zone has a maximum value Vr,max which is smaller than 20 cm/min. The temperature in a rear heating portion of the heating zone, assigned to the end of the deformation zone, is lower than in a front heating portion assigned to the beginning of the deformation zone.

Method for producing a tube of glass

A method for producing a component includes joining individual wall parts, especially for producing a melting crucible for use at a high operating temperature in a crucible-pulling method for quartz glass, wherein at least two wall parts of a refractory metal or of a base alloy of a refractory metal are provided, butt-joined to form a joint and joined together by sintering at a temperature above 1500&#xb0; C. to form the component. A sealant is inserted into the joint to provide a component of improved tightness and to ensure improved sintering of the individual parts of the component. A component produced according to the method, particularly a melting crucible, particularly in a crucible pulling method for quartz glass, has the joint between the butt-joined walls closed in a gas-tight manner by a sealant.

Method for producing a component, particularly for use in a crucible pulling method for quartz glass

A method for forming a hollow cylinder, in a single step or in as small a number of steps as possible, into a quartz glass tube with a large outer diameter and high dimensional stability is provided. The cylinder, while rotating about a rotation axis, is softened in portions in a heating zone which is moved at a relative feed rate Va, and the softened portion is radially expanded by a centrifugal force and/or an internal overpressure applied in the hollow cylinder bore so as to form a deformation zone. The tube is continuously shaped with an outer diameter Dwhich is greater than that of the hollow cylinder D. The radial expansion of the softened portion is carried out at a location-dependent radial expansion rate Vr, the profile of which along the deformation zone has a maximum value Vr,max which is smaller than two times the feed rate Va.

In a known process for drawing a quartz glass strand, SiOparticles are fed to a melting crucible and softened therein to form a quartz glass mass, and the softened quartz glass mass is pulled vertically downward as a quartz glass strand via a drawing nozzle which is provided in the bottom region of the melting crucible and has a gap-like drawing nozzle opening. In order, on the basis thereof, to make it easier to reproducibly produce a quartz glass strand with a minor deviation from the nominal wall thickness profile, and in particular to avoid irregularly occurring indentations and protrusions of the wall thickness profile, it is proposed according to the invention that the wall thickness profile of the quartz glass strand is detected, and that the drawing nozzle is heated by means of a plurality of heating elements which are distributed around the drawing nozzle opening and can be electrically actuated independently of one another, and that the quartz glass mass is locally heated by means of the heating elements within the gap-like drawing nozzle opening depending on measurement results of the wall thickness profile.

Method and apparatus for drawing a quartz glass strand

In a known drawing method for producing a cylindrical component from quartz glass, a quartz glass strand () is continuously drawn off from a softened quartz glass composition () vertically downwards in the drawing direction (), a piece () with a weight G is detached from the free end of the strand at a time tand the cylindrical component is produced from the piece (). When the piece () is detached, there may be a sudden reduction in weight, which leads to fluctuations in the thawing-off control. To counteract this, it is proposed according to the invention that a weight compensating force which acts counter to the drawing direction (), increases over time and completely or partially compensates for the weight G of the piece (), is applied to the piece to be detached at a time tbefore t

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Aschaffenburg, Germany

Boris Gromann