Tsinghua University

Nuctech Company Limited

China National Petroleum Corporation

China University of Petroleum

Bing Feng

Ziran Zhao

Yingxin Wang

Zhiqiang Chen

Li Ni Zhang

Yuanjing Li

Jing Li

Baojian Shen

Zhuoyan Liu

Dongmei Yu

Bojun Shen

Zhihua Zhang

Xiaohua Wang

Yinpeng Liang

Wencheng Zhang

Qiaoxia Guo

Guangming Wen

Ran Tian

The present invention relates to a synthesis method for ETS-10 titanosilicate molecular sieves. The method comprises the steps of mixing a titanium oxide hydrosol, a silicon source, a sodium hydroxide, a fluorine-containing mineralizer and a water to give a gel and adjusting the pH thereof to 10.4 to 10.8; and hydrothermal crystallizing the gel at 170 to 250&#xb0; C. for 10 to 100 hours to obtain the ETS-10 titanosilicate molecular sieves. In the synthesis method for ETS-10 titanosilicate molecular sieves provided by the present invention, a titanium oxide hydrosol is used as the titanium source to synthesize the ETS-10 titanosilicate molecular sieves, and the problem that conventional soluble titanium salt-based titanium sources tend to hydrolyze and the problem of poor dispersibility for the titanium source system of insoluble titanium oxide are therefore prevented. The ETS-10 titanosilicate molecular sieves synthesized has high purity and high crystallinity.

Synthesis method for ETS-10 titanosilicate molecular sieve

A method and an apparatus for measuring terahertz time-domain spectrum, which relate to the field of terahertz time-domain spectrum. The method comprises the steps of: generating a first pulse laser beam from a first femtosecond laser device at a preset repetition frequency to generate THz pulses; generating a second pulse laser beam from a second femtosecond laser device at the repetition frequency; measuring electric field intensities of the THz pulses at respective phase differences between the first pulse laser beam and the second pulse laser beam; and obtaining a THz time-domain spectroscopy by performing Fourier transformation of data representative of the electric field intensities. THz spectrum measured according to the method and apparatus improves spectroscopy resolution and provides a broader detection range.

Method and apparatus for measuring terahertz time-domain spectroscopy

The present invention relates to a method for assessing the purity of vegetable oils by means of THz time-domain spectroscopy, comprising the steps of: measuring the THz time-domain spectra of standard vegetable oils to establish a spectral database; measuring the THz time-domain spectrum of vegetable oil to be detected; analyzing the purity of the detected vegetable oil based on the pre-built database. The present invention also relates to an apparatus for assessing purity of vegetable oil by means of THz time-domain spectroscopy, comprising: spectrum measuring device for measuring time-domain waveforms of THz pulses before and after transmitting the vegetable oil held in a container by transmission approach, or directly measuring time-domain waveforms of THz pulses before and after reflecting from the vegetable oil by reflection approach; and data processing device for extracting physical parameters of the vegetable oil in THz region according to the time-domain waveforms. Compared with the prior art, the method according to the present invention is easy, rapid and quantitative.

Method and apparatus for assessing purity of vegetable oils by means of terahertz time-domain spectroscopy

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Beijing, China

Bing Feng