US Government as Represented by the Secretary of the Army

USA as Represented by Secretary of the Navy

Anthony P Shaw

Jay C Poret

Lori J Groven

Jason Brusnahan

Zhaohua Luan

Lauren Morris

Christopher D Haines

Joshua Koenig

Christopher Csernica

Christina M Yamamoto

Eric J Miklaszewski

The present invention relates to methods of preparing pre-mixed compositions that can be combined to form pyrotechnic compositions. In exemplary embodiments, a binder ingredient is premixed with the pyrotechnic fuels and can also include other pyrotechnic additives and processing aides. Other binder ingredients can be premixed with the pyrotechnic oxidizers and can also include other pyrotechnic additives and processing aides. The resulting mixtures are not explosive and are therefore easier to store and much safer to handle. These pre-mixed mixtures can be stored in bulk until needed and rapidly combined to achieve final composition.

Three part mixing process for energetic materials and epoxy binder

The present invention is a pyrotechnic time delay system that is improved over prior-art designs. Specifically, the system described herein comprises at least one delay element. The delay element or delay elements each have an input charge, a delay composition, and an output charge. Both the input charge and the output charge are igniter compositions and are comprised of the same components despite having different functional goals. The input charge and output charge compositions preferably contain titanium, manganese dioxide, and polytetrafluoroethylene. The delay composition may be modified from current formulations to include manganese and manganese dioxide, or tungsten and manganese dioxide. The system disclosed herein may be comprised of one delay element, or it may be modular wherein multiple delay elements are connected in series.

Pyrotechnic delay element device

The present invention is a pyrotechnic time delay system that is improved over prior-art designs. Specifically, the system described herein comprises at least one delay element. The delay element or delay dements each have an input charge, a delay composition, and an output charge. Both the input charge and the output charge are igniter compositions and are comprised of the same components despite having different functional goals. The input charge and output charge compositions preferably contain titanium, manganese dioxide, and polytetrafluoroethylene. The delay composition may be modified from current formulations to include manganese and manganese dioxide, or tungsten and manganese dioxide. The system disclosed herein may be comprised of one delay element, or it may be modular wherein multiple delay elements are connected in series.

A novel pyrotechnic composition comprising nanostructured crystalline boron phosphide and oxidizer such as potassium nitrate wherein the crystalline boron phosphide is synthesized by a self-propagating high-temperature reaction. The nanostructured crystalline boron phosphide and oxidizer pyrotechnic composition unexpectedly emits smoke and green flame upon ignition.

Pyrotechnic compositions comprising nanostructured crystalline boron phosphide and oxidizer

A simplified method for synthesizing boron phosphide at high yields. The method requires mixing of boron phosphate and magnesium metal without diluents into a homogenous mixture, loosely packing the mixture at less than 20,000 psi and igniting the mixture using an energy input that is not greater than 20% of the reaction energy output to create a self-propagating high-temperature reaction wherein the boron phosphate and magnesium metal is completely burned during the reaction to synthesize boron phosphide at high yields.

High-yield synthesis of nanostructured boron phosphide by a pyrotechnic method

A precise, slow burning, pyrotechnic delay composition composed of a ternary system of from about 8 to about 55 weight percent BC fuel, 35 to about 82 weight percent NalOoxidizer, and PTFE which acts as a pyrotechnic oxidizer and lubricant&#x2014;such that the resulting composition has surprisingly good mechanical properties, i.e. it can be pressed to a desirably high consolidated density with ordinary loading force, and with minimal wear on the tooling used for pressing.

Boron carbide pyrotechnic time delay

An environmentally safe, nontoxic energetic time delay composition useful in small diameter aluminum tubes (i.e., typical military delay housings), which provides desired delay propagation rates of from less than about 2 to about 38 mm/s through such delay housings&#x2014;the compositions being compressed stoichiometric mixes of Ti and C powders; Ni and Al powders; a combination of Ti/C and 3Ni/Al powders; and a combination of Ti/C and Ni/Al powders, diluted with inert alumina.

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Madison, NJ, United States of America

Anthony P Shaw