Occidental Research Corporation

Occidental Chemical Company

Occidental Chemical Corporation

Allen S Adams

John D Ellis

Michael B Caesar

F Michael Gragg

Fredrick M Gragg

An apparatus useful for the preparation of phosphoric acid from phosphate rock and a strong acid, comprises a closed vessel, a draft tube, means connected to the inner walls of said vessel amd mounting said draft tube in a vertical position within said vessel, an agitator positioned within said draft tube, a shaft for said agitator mounted axially of said vessel and extending into said draft tube, an inlet conduit to said vessel for introducing a feed slurry (e.g. phosphate rock and strong acid) into said vessel, said inlet conduit preferably having a lower end portion terminating within said draft tube and wherein, said draft tube has an outwardly flared lower skirt portion terminating in the bottom portion of said vessel, and preferably including a vent pipe connected to said inlet conduit to reduce foaming generated by the reaction in said vessel and to prevent blockage of said inlet conduit, and including means for applying air, under pressure, to the bottom of said reactor and/or under the bottom of said lower skirt portion, to prevent settling of undissolved solids.

Apparatus for reacting a particulate solid and a liquid

A system for the preparation of phosphoric acid from phosphate rock and sulfuric acid, includes in combination a first reaction vessel containing a first slurry comprising calcium sulfate hemihydrate, monocalcium phosphate and phosphoric acid, a second reaction vessel containing a second slurry comprising calcium sulfate hemihydrate, circulation means including a draft tube disposed centrally in each of said vessels and an agitator positioned axially in each of said vessels within said draft tube, a first conduit interconnecting said first and second reaction vessels for conducting said first slurry from said first reaction vessel to said second reaction vessel, a second conduit interconnecting said vessels for conducting said second slurry from said second reaction vessel to said first reaction vessel, an inlet pipe for introducing phosphate rock and phosphoric acid to said first reaction vessel, and wherein a vent is connected to said inlet pipe to permit escape of gases and, thus, increasing the rate of flow of said phosphate rock and phosphoric acid to said first reaction vessel.

Feed system for phosphoric acid production with decreased foaming

A system for the preparation of phosphoric acid from phosphate rock and sulfuric acid, includes in combination a first reaction vessel containing a first slurry comprising calcium sulfate hemihydrate, monocalcium phosphate and phosphoric acid, a second reaction vessel containing a second slurry comprising calcium sulfate hemihydrate, circulation means including a draft tube disposed centrally in each of said vessels and an agitator positioned axially in each of said vessels within said draft tube, a first conduit interconnecting said first and second reaction vessels for conducting said first slurry from said first reaction vessel to said second reaction vessel, a second conduit interconnecting said vessels for conducting said second slurry from said second reaction vessel to said first reaction vessel, an inlet pipe for introducing phosphate rock and phosphoric acid to said first reaction vessel, said inlet pipe connected with the interior of said draft tube in said first vessel and wherein a vent is connected to said inlet pipe to permit escape of gases and, thus, increasing the rate of flow of said phosphate rock and phosphoric acid to said first reaction vessel.

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Jasper, FL, United States of America

Allen S Adams