Bodenseewerk Perkin-Elmer Gmbh

Perkinelmer Instruments LLC

Albert Gilmutdinov

Michael Sperling

Bernhard Welz

The present invention refers to a method for atomic absorption spectroscopy of an analyte which is contained in a sample to be analyzed and which is converted into free atoms in an absorption volume of an atomizer, said method comprising the steps of (a) position- and time-dependent measuring of the atomic absorption over the cross-section of the absorption volume and (b) simultaneous determination of surface temperatures of the atomizer. This method is characterized by the steps of (c) reconstructing the temperature field in said absorption volume on the basis of the surface temperatures determined, (d) determining position- and time-dependent numbers of particles of the absorbing atoms of the analyte on the basis of the measurements of the position- and time-dependent atomic absorption and the absorption profile that has been determined with due regard to effects influencing the line profile of the analyte and with due regard to the reconstructed temperature field, and (e) determining the time-dependent total number of the absorbing atoms of the analyte on the basis of the position- and time-dependent numbers of particles. In addition, the present invention concerns a device for carrying out this method.

Method and a device for atomic absorption spectroscopy

An electrically heatable hollow-body furnace with a secondary surface on which an analyte of a sample can be condensed prior to being atomized. The furnace is constructed in two sections which are capable of being electrically heated independently of one another. The secondary surface is defined by a surface of one of the sections. A process for atomizing an analyte of a sample to be examined, utilizing the device according to the following steps: introducing the sample into a hollow-body furnace having a secondary surface, condensing the analyte on the secondary surface and atomizing the analyte.

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Kazan, Russia

Albert Gilmutdinov